Reductive acylation[有化] 还原酰化;翻译
double acylation二酰化
acylation reactions酰化反应
acylation method酰化法
tra acylation转酰基作用
amine acylation胺酰化
enzymatic acylation酶促酰化反应
intramolecular acylation分子内苯环上的酰基化反应
selective acylation选择性酰化
In this paper, a new simple and efficient synthesis method of N-acetyl amines was found. Which use the cheap and commercially available ethyl ester as the acylation reagent, aluminum chloride and triethylamine as promoter.
本文以芳胺化合物的乙酰化方法为研究对象,通过深入研究,发现了一种全新的、简便高效的芳胺化合物乙酰化方法,即:利用氯化铝和三乙胺作为促进剂,用价廉易得的乙酸乙酯作为酰化试剂对芳胺进行乙酰化反应。
N-(3-Methyl-piperidin-4-yl)-N-phenyl-propionamide was synthesized with aniline,sodium borohydride,propionyl chloride and pd/c,via condensation reaction, reduction reaction,acylation reaction and debenzylation.
中间体N-3-甲基-4-哌啶基-N-丙酰苯胺的合成以1-苄基-3-甲基哌啶酮为起始原料,经过与苯胺缩合反应,硼氢化钠还原,丙酰氯酰基化和钯碳催化脱苄基等四步反应。
The synthesis method contains four steps including the esterification, the thiosulfate reaction, the acylation and the acidification. With high purity, the yield reached 53%.
以截短侧耳素为原料,采用四步反应合成法,通过酯化,硫代、酰胺化、酸化成盐得到产物,收率均可达53%。
参考来源 - 几种抗生素药物及中间体的合成研究N（名词） the introduction into a chemical compound of an acyl group 酰化