furoin acetate糠偶姻乙酸酯
monoester of furoin糠偶姻单酯
Novel Synthesis of Furoin糠偶姻的制备
The experimental results show the best synthesis conditions:furoin 20 mmol,n(furoin)∶n(acid chloride)=1∶2.2,triethylanine 25 mL,power of microwave 240 W and radiation time 10 min. Yields of the products were over 94%.
实验结果表明:当糠偶姻的用量为20 mmol时,最适宜反应条件为:n(糠偶姻)∶n(酰氯)=1∶2.2,有机碱三乙胺的用量为25 mL,微波工作功率为240 W,辐射时间10 min,产率94%以上。
参考来源 - 微波辐射下1